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Beilstein J. Org. Chem. 2017, 13, 329–337, doi:10.3762/bjoc.13.36
Graphical Abstract
Scheme 1: Target reaction – intramolecular cyclisation of 1 followed by N-methylation with methanol to yield ...
Figure 1: Simplified schematic demonstrating a self-optimising reactor [34,35,37,44]. The reagents are pumped into the sys...
Figure 2: Result of the SNOBFIT optimisation for N-methylpiperidine (2b) with and without CO2 showing yields ...
Scheme 2: Cyclisation and N-alkylation of 1,4- and 1,6-amino alcohols.
Scheme 3: a) Reactions highlighting the incorporation of CO2 in to 16. b) High temperature reaction of 15 yie...
Scheme 4: Summary of products obtained from the reactions of amino alcohols over γ-Al2O3 in scCO2.
Figure 3: Diagram of the high pressure equipment used in the experiments.